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KITALYSIS-RCM

KitAlysis™ High-Throughput Medium (5, 6, 7) Ring Closing Metathesis Reaction Screening Kit - Pack of 2

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제품정보 (DICE 배송 시 비용 별도)

NACRES:
NA.22
UNSPSC Code:
12161600
기술 서비스
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도움 문의

product line

KitAlysis™

reaction suitability

core: palladium, reaction type: Buchwald-Hartwig Cross Coupling Reaction, reaction type: Heck Reaction, reaction type: Hiyama Coupling, reaction type: Negishi Coupling, reaction type: Sonogashira Coupling, reaction type: Stille Coupling, reaction type: Suzuki-Miyaura Coupling

storage temp.

2-8°C

Application

Screening kit for ring closing metathesis. Step-by-step user guides and a downloadable experimental excel sheets are provided in the below hyperlinks.

Step-by-Step Guide for Ring Closing Metathesis/Cross Metathesis Reaction Screening Kit

Downloadable experimental excel file

Each kit contains 2 customizable screening sets that include the following components:
  • 6x4 pre-weighed catalysts in glass microvials loaded with stir bars and topped with cap mat.
  • 2 (2 mL) ampules each of of ClPh, PhMe, i-PrOAc, Me-THF, and TFA.
  • 1 KitAlysis 24-well reaction block replacement film.
  • 4 empty substrate stock solution reaction vials with stir bars.
  • 1 internal standard.
Monitor reaction progress via TLC-MS by following this protocol

Best when used with KitAlysis Benchtop Inertion Box and 24-well Reaction Block (sold separately).

Features and Benefits

  • Designed and tested by synthetic chemists.
  • Easily run 24-microscale reaction in parallel.
  • 20 μmol reactions with 1 μmol catalyst (5 mol%), 0.2 M concentration, and optional TFA additive.
  • Customizable and downloadable excel template for quick calculations and easy incorporation into electronic laboratory notebooks.

Legal Information

KitAlysis is a trademark of Sigma-Aldrich Co. LLC

키트 구성품 전용

제품 번호
설명
  • SnapIT Ampule Opener, Regular, for 1-2ml, 5-10ml, 10-15ml ampoules 1 EA

키트 구성품 역시 별도로 이용 가능함

제품 번호
설명
SDS & 가격
  • 569747
    Grubbs Catalyst® M204, Umicore 3 µmol
    SDS
  • 569755
    Hoveyda-Grubbs Catalyst® M720, Umicore, 97% 3 µmol
    SDS
  • 579726
    Grubbs Catalyst® M102, Umicore, 97% 3 µmol
    SDS
  • 682365
    Grubbs Catalyst® M207, Umicore 3 µmol
    SDS
  • 682373
    Hoveyda-Grubbs Catalyst® M721, Umicore 3 µmol
    SDS
  • 729345
    Hoveyda-Grubbs Catalyst® M722, Umicore 3 µmol
    SDS
  • 900519
    Isopropyl acetate, anhydrous, ZerO2®, ≥99.6% 8 mL
    SDS
모두 보기 (11)

signalword

Danger

Hazard Classifications

Acute Tox. 4 Inhalation - Acute Tox. 4 Oral - Aquatic Acute 1 - Aquatic Chronic 1 - Asp. Tox. 1 - Eye Dam. 1 - Flam. Liq. 2 - Repr. 2 - Skin Irrit. 2 - STOT RE 2 Inhalation - STOT SE 3

target_organs

Central nervous system, Respiratory system

supp_hazards

EUH019

저장 등급

3 - Flammable liquids

wgk

WGK 3

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시험 성적서(COA)

Lot/Batch Number

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프로토콜

Catalyst Screening & TLC-MS for Reaction Analysis

Catalyst screening kits, KitAlysis™, and TLC-MS analysis enable high-throughput synthesis and analysis for efficient reactions.

문서

KitAlysis™ High-Throughput Screening Platform

KitAlysis High-Throughput Screening Kits provide solution to efficiently identify or optimize suitable catalytic reaction conditions. Chemist can rapidly run 24 unique micro scale reactions in parallel with tailored conditions.

관련 콘텐츠

반응 설계 및 최적화

유기 합성의 화학 반응 설계 및 최적화는 반응 파라미터를 정밀하게 변경하여 표적 분자에 대한 경로를 찾는 데 최적의 결과를 얻는 것을 목표로 합니다.

Olefin Metathesis Application Guide

The Olefin Application Metathesis Application Guide provides - The Key Features of Metathesis, General Reaction Procedures, Guidance for Choosing the Correct Metathesis Route, A Metathesis Quick Guide

Reaction Design & Optimization

Chemical reaction design and optimization in organic synthesis aims to precisely alter reaction parameters to achieve optimum results in finding pathways to target molecules.

관련 콘텐츠 모두 보기
High-Throughput Experimentation in Catalysis and Materials Science.
Gordillo A, et al.
Ullmann's Encyclopedia of Industrial Chemistry (2014)
Scientist-Led High-Throughput Experimentation (HTE) and Its Utility in Academia and Industry.
Schmink JR, et al.
Aldrichimica Acta, 46, 71-80 (2013)
Spencer D Dreher et al.
Journal of the American Chemical Society, 130(29), 9257-9259 (2008-06-28)
Microscale parallel experimentation was used to discover three catalyst systems capable of coupling secondary organotrifluoroborates with sterically and electronically demanding aryl chlorides and bromides. The ensuing results represent the first comprehensive study of alkylboron coupling to aryl chlorides and, in
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국제 무역 품목 번호

SKUGTIN
KITALYSIS-RCM-2PK04061833690352
KITALYSIS-RCM-2PAK04061833690345