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KITALYSISBASE

KitAlysis High-Throughput Base Screening Kit - Pack of 2

Synonyme(s) :

Base screen, Base screening kit, KitAlysis base

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A propos de cet article

NACRES:
NA.22
UNSPSC Code:
12161600
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product line

KitAlysis

reaction suitability

reaction type: Buchwald-Hartwig Cross Coupling Reaction, reaction type: Cross Couplings, reaction type: Heck Reaction, reaction type: Hiyama Coupling, reaction type: Negishi Coupling, reaction type: Sonogashira Coupling, reaction type: Stille Coupling, reaction type: Suzuki-Miyaura Coupling

functional group

phosphine

Application

Versatile base screening kit for cross-coupling reactions and other synthetic transformations. Step-by-step user guide and a downloadable experimental excel sheet are provided in the below hyperlinks.

Step-by-Step Guide for KitAlysis High-Throughput Base Reaction Screening Kit

Downloadable experimental excel file

Each kit contains 2 customizable screening sets that contain the following:
  • 7 X 2 pre-weighed bases (30 μmol) in individual microvials with magnetic stir bars
  • 4 X 2 base solutions
  • 2 empty microvials for Chemist′s Choice of base allowing customization
  • 4 degassed anhydrous solvents (DMF, MeOH, THF, Toluene)
  • 2 NEW KitAlysis 24-Well Reaction Block Replacement Films
  • 4 empty substrate stock solution reaction vials with stirbars
Monitor reaction progress via TLC-MS by following this protocol

Best when used with KitAlysis Benchtop Inertion Box and 24-well Reaction Block (sold separately).

Features and Benefits

  • Designed and tested by synthetic chemists
  • Easily run 24-microscale reactions in parallel
  • 10 μmol reactions with 3 equiv. base, 0.1 M concentration
  • Customizable Excel Template for quick calculations and easy incorporation into electronic laboratory notebooks

Legal Information

KitAlysis is a trademark of Sigma-Aldrich Co. LLC


Composants de kit seuls

Réf. du produit
Description

  • Potassium bicarbonate, ACS reagent, 99.7%, powder, crystals or granules

Composants de kit également disponibles séparément

Réf. du produit
Description
FDS & Tarif

  • Potassium phosphate tribasic, anhydrous, free-flowing, Redi-Dri, reagent grade, ≥97%
    FDS

  • Cesium carbonate, ReagentPlus®, 99%
    FDS

  • Potassium hydroxide, ≥99.95% trace metals basis
    FDS

  • Potassium acetate, anhydrous, free-flowing, Redi-Dri, ACS reagent, ≥99.0%
    FDS

  • 1,8-Diazabicyclo[5.4.0]undec-7-ene, 98%
    FDS

  • Lithium bis(trimethylsilyl)amide solution, 1.0 M in THF
    FDS

  • Sodium tert-butoxide solution, 2 M in THF, ZerO2®
    FDS

Afficher tout (16)

signalword

Danger

Hazard Classifications

Acute Tox. 3 Dermal - Acute Tox. 3 Inhalation - Acute Tox. 3 Oral - Aquatic Chronic 3 - Asp. Tox. 1 - Carc. 2 - Eye Dam. 1 - Flam. Liq. 2 - Repr. 1B - Self-heat. 1 - Skin Corr. 1A - STOT RE 2 Inhalation - STOT SE 1 - STOT SE 3

Classe de stockage

4.1B - Flammable solid hazardous materials

flash_point_f

-5.8 °F

flash_point_c

-21 °C

wgk

WGK 2

target_organs

Central nervous system, Eyes,Central nervous system, Respiratory system

supp_hazards



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Articles

KitAlysis High-Throughput Screening Kits provide solution to efficiently identify or optimize suitable catalytic reaction conditions. Chemist can rapidly run 24 unique micro scale reactions in parallel with tailored conditions.

Contenu apparenté

Chemical reaction design and optimization in organic synthesis aims to precisely alter reaction parameters to achieve optimum results in finding pathways to target molecules.

La conception et l'optimisation d'une réaction chimique en synthèse organique vise à altérer avec précision certains paramètres de la réaction pour obtenir des résultats optimaux dans la recherche de voies menant aux molécules cibles.

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Numéro d'article de commerce international

RéférenceGTIN
KITALYSISBASE-2PK04061835443031