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271012

N,N-Dimethylacetamide

Name: <I>N,N</I>-Dimethylacetamide
Brand: SIAL

anhydrous, 99.8%

동의어(들):

DMAc

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제품정보 (DICE 배송 시 비용 별도)

Linear Formula:

CH₃CON(CH₃)₂

CAS 번호:

127-19-5

Molecular Weight:

87.12

UNSPSC Code:

12352111

NACRES:

NA.21

PubChem Substance ID:

57648218

EC Number:

204-826-4

Beilstein/REAXYS Number:

1737614

MDL number:

MFCD00008686

Assay:

99.8%

Grade:

anhydrous

Bp:

164.5-166 °C (lit.)

Vapor pressure:

2 mmHg ( 25 °C), 4 mmHg ( 38 °C)

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도움 문의

속성

grade

anhydrous

Quality Level

300

vapor density

3 (vs air)

vapor pressure

2 mmHg ( 25 °C), 4 mmHg ( 38 °C)

assay

99.8%

form

liquid

autoignition temp.

914 °F

expl. lim.

1.8 %, 100 °F, 11.5 %, 160 °F

impurities

<0.005% water

evapn. residue

<0.001%

refractive index

n20/D 1.437 (lit.)

pH

4 (20 °C, 200 g/L)

bp

164.5-166 °C (lit.)

mp

−20 °C (lit.)

density

0.937 g/mL at 25 °C (lit.)

SMILES string

CN(C)C(C)=O

InChI

1S/C4H9NO/c1-4(6)5(2)3/h1-3H3

InChI key

FXHOOIRPVKKKFG-UHFFFAOYSA-N

설명

Application

N,N-Dimethylacetamide may be used as a solvent in the following processes:

Palladium (II) acetate-butyldi-1-adamantylphosphine catalyzed arylation of 2-isobutylthiazole with chlorobenzene to form 5-phenyl-2-isobutylthiazole.
Synthesis of β-, γ-, and δ-metallo ester intermediates that can react with acid chlorides to form γ-, δ-, and ε-keto esters.
Synthesis of (R)-(-)-methyl 1,1′-binaphthyl-2,2′-diylphosphate that can be used as a precursor for preparing (R)-(+)-1,1′-binaphthalene-2,2′-diol.

Packaging

View returnable container options.

Other Notes

The article number 271012-4X2L will be discontinued. Please order the single bottle 271012-2L which is physically identical with the same exact specifications.

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pictograms

GHS08,GHS07

signalword

Danger

hcodes

H312 + H332,H319,H360D

pcodes

P202 - P280 - P302 + P352 + P312 - P304 + P340 + P312 - P305 + P351 + P338 - P308 + P313

Hazard Classifications

Acute Tox. 4 Dermal - Acute Tox. 4 Inhalation - Eye Irrit. 2 - Repr. 1B

저장 등급

6.1C - Combustible acute toxic Cat.3 / toxic compounds or compounds which causing chronic effects

flash_point_f

147.2 °F - closed cup

flash_point_c

64 °C - closed cup

ppe

Eyeshields, Faceshields, Gloves, type ABEK (EN14387) respirator filter

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문서

Scale-Up Guide: Buchwald-Hartwig Amination

Preformed catalysts in the kit are stable but become air-sensitive when activated; Schlenk technique aids scale-up.