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MilliporeSigma

57051

Supelclean LC-Si SPE Tube

bed wt. 1 g, volume 6 mL, pkg of 30 ea

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About This Item

UNSPSC Code:
41115712
NACRES:
NB.21
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Quality Level

material

PE frit, polypropylene hardware

product line

Supelclean

composition

bed wt., 1 g

packaging

pkg of 30 ea

technique(s)

solid phase extraction (SPE): suitable

surface area

475 m2/g

volume

6 mL

matrix

silica gel base material (irregularly shaped)

matrix active group

silica bonding

particle size

45 μm

pore size

0.8 cm3/g pore volume, 60 Å pore size

application(s)

food and beverages

separation technique

normal phase

General description

Supelclean LC-Si SPE tube is used to extract polar analytes from nonpolar samples.

Application

Supelclean LC-Si SPE Tube may be used for the solid-phase extraction of:
  • Phospholipids in dairy products prior to their determination by high performance liquid chromatography-evaporative light scattering detector (HPLC-ELSD).
  • Free and esterified sterols in Portuguese olive oils prior to their estimation by gas chromatography-mass spectrometry (GC-MS).
  • Synthetic musks in cream prior to their quantification by GC combined with tandem mass spectrometry (MS/MS).
  • Phospholipids in milk samples prior to their quantification by hydrophilic interaction liquid chromatography (HILIC) in conjunction with ELSD as well as ion trap-time-of-flight mass spectrometry (IT-TOF MS).

Legal Information

Supelclean is a trademark of Sigma-Aldrich Co. LLC


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Storage Class

11 - Combustible Solids

wgk

nwg

flash_point_f

Not applicable

flash_point_c

Not applicable



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Protocols

(soybean), ≥97%; L-α-Phosphatidylethanolamine from egg yolk, Type III, ≥97% (TLC), lyophilized powder; L-α-Phosphatidylcholine, from egg yolk, Type XVI-E, ≥99% (TLC), lyophilized powder; Sphingomyelin, from chicken egg yolk, ≥95%


Determination of phospholipids in milk samples by means of hydrophilic interaction liquid chromatography coupled to evaporative light scattering and mass spectrometry detection.
Donato P, et al.
Journal of Chromatography A, 1218(37), 6476-6482 (2011)
Quantification of free and esterified sterols in Portuguese olive oils by solid-phase extraction and gas chromatography-mass spectrometry.
Cunha SS, et al.
Journal of Chromatography A, 1128(1-2), 220-227 (2006)
Analysis of 7 synthetic musks in cream by supported liquid extraction and solid phase extraction followed by GC-MS/MS.
Dong H, et al.
Talanta, 120(1-2), 248-254 (2014)



Global Trade Item Number

SKUGTIN
5705104061833667934