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Merck

KITALYSIS-SM

KitAlysis High-Throughput Suzuki-Miyaura Cross-Coupling Reaction Screening Kit - Pack of 4

동의어(들):

Suzuki-Miyaura Cross-Coupling

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제품정보 (DICE 배송 시 비용 별도)

NACRES:
NA.22
UNSPSC Code:
12161600
기술 서비스
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도움 문의


product line

KitAlysis

reaction suitability

reaction type: Cross Couplings, reaction type: Suzuki-Miyaura Coupling, reagent type: catalyst
core: palladium

functional group

phosphine

Application

Screening kit for Suzuki-Miyaura cross-coupling reaction. Step-by-step user guide and a downloadable experimental excel sheets are provided in the below hyperlink.
Step-by-Step Guide for Suzuki-Miyaura Cross-Coupling Reaction Screening Kit
Downloadable experimental excel sheet

Each kit contains 4 customizable screening sets that include the following components:
  • 6 x 4 pre-weighed catalysts in glass vials loaded with stir bars and topped with cap mat.
  • 1 (2 mL) ampule each of Toluene, THF, n-Butanol, DMAc, and aq. 1.5 M K3PO4.
  • 4 NEW KitAlysis 24-Well Reaction Block Replacement Films.
  • 4 substrate reaction vials with stir bars.
  • 1 internal standard.
Monitor reaction progress via TLC-MS by following this protocol

Best when used with KitAlysis Benchtop Inertion Box and 24-well Reaction Block (sold separately).

Features and Benefits

  • Designed and tested by synthetic chemists.
  • Easily run 24-microscale reactions in parallel.
  • 10 μmol reactions with 1 μmol catalyst, 3 equiv. base, 0.1 M concentration.
  • Customizable Excel Template for quick calculations and easy incorporation into electronic laboratory notebooks.

Legal Information

KitAlysis is a trademark of Sigma-Aldrich Co. LLC


키트 구성품 전용

제품 번호
설명

  • SnapIT Ampule Opener, Regular, for 1-2ml, 5-10ml, 10-15ml ampoules 1 EA

키트 구성품 역시 별도로 이용 가능함

제품 번호
설명
SDS & 가격

  • Pd-PEPPSI-IPent catalyst, ≥95% 5 µmol
    SDS

  • SPhos Pd G2 5 µmol
    SDS

  • cataCXium® A Pd G2 5 µmol
    SDS

  • XPhos Pd G3, 98%, 1:1 MTBE adduct 5 µmol
    SDS

  • P(Cy3) Pd G3, 97% 5 µmol
    SDS

  • APhos Pd G3, 97% 5 µmol
    SDS

  • Toluene, anhydrous, ZerO2®, 99.8% 8 mL
    SDS

모두 보기 (12)

signalword

Danger

target_organs

Central nervous system, Respiratory system

supp_hazards

저장 등급

3 - Flammable liquids

flash_point_f

1.4 °F

flash_point_c

-17 °C

wgk

WGK 3

Hazard Classifications

Acute Tox. 4 Dermal - Acute Tox. 4 Inhalation - Acute Tox. 4 Oral - Aquatic Acute 1 - Aquatic Chronic 1 - Asp. Tox. 1 - Carc. 2 - Eye Dam. 1 - Flam. Liq. 2 - Repr. 1B - Skin Irrit. 2 - STOT RE 2 Inhalation - STOT SE 3



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시험 성적서(COA)

Lot/Batch Number

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이 제품을 이미 가지고 계십니까?

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문서 라이브러리 방문


프로토콜

A step-by-step protocol guide for KitAlysis Suzuki-Miyaura Cross-Coupling Reaction Screening Kit.

문서

KitAlysis High-Throughput Screening Kits provide solution to efficiently identify or optimize suitable catalytic reaction conditions. Chemist can rapidly run 24 unique micro scale reactions in parallel with tailored conditions.

Tools aid in kit setup for organic chemistry techniques, ensuring ease and success.

All of the preformed catalysts used in the kit are air and moisture stable complexes in their commercially available form.

모든 기사 보기

관련 콘텐츠

유기 합성의 화학 반응 설계 및 최적화는 반응 파라미터를 정밀하게 변경하여 표적 분자에 대한 경로를 찾는 데 최적의 결과를 얻는 것을 목표로 합니다.

Chemical reaction design and optimization in organic synthesis aims to precisely alter reaction parameters to achieve optimum results in finding pathways to target molecules.

관련 콘텐츠 모두 보기

High-Throughput Experimentation in Catalysis and Materials Science.
Gordillo A, et al.
Ullmann's Encyclopedia of Industrial Chemistry (2014)
Scientist-Led High-Throughput Experimentation (HTE) and Its Utility in Academia and Industry.
Schmink JR, et al.
Aldrichimica Acta, 46, 71-80 (2013)
Spencer D Dreher et al.
Journal of the American Chemical Society, 130(29), 9257-9259 (2008-06-28)
Microscale parallel experimentation was used to discover three catalyst systems capable of coupling secondary organotrifluoroborates with sterically and electronically demanding aryl chlorides and bromides. The ensuing results represent the first comprehensive study of alkylboron coupling to aryl chlorides and, in



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SKUGTIN
KITALYSIS-SM-4PAK04061833553756