KITALYSIS-CN
KitAlysis™ High-Throughput Buchwald-Hartwig Amination Reaction Screening Kit-Pack of 4
Synonym(s):
Amination Screening Kit, Buchwald-Hartwig Amination
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About This Item
product line
KitAlysis™
reaction suitability
reaction type: Buchwald-Hartwig Cross Coupling Reaction, reaction type: Cross Couplings, reagent type: catalyst
core: palladium
storage temp.
room temp
General description
Application
Two Solvents, Weak Base (Cs2CO3)
Download the experimental excel file here
Two Solvents, Strong Base (NaOt-Bu)
Download the experimental excel file here
One Solvent (Dioxane), Two Bases
Download the experimental excel file here
One Solvent (DMAc), Two Bases
Download the experimental excel file here
Each kit contains 4 screening sets that contain the following:
Each customizable screening kit contains
- 12 X 2 pre-weighed catalysts (1 μmol) in individual microvials with magnetic stir bars
- 2 bases (NaOt-Bu and Cs2CO3)
- 2 degassed anhydrous solvents (dioxane and DMAc) in ampules
- 2 substrate reaction vials with stir bars
- 1 internal standard
- 4 reaction block replacement films
Best when used with KitAlysis Benchtop Inertion Box and 24-well Reaction Block (sold separately).
Features and Benefits
- Designed and tested by synthetic chemists
- Easily run 24-microscale reaction in parallel
- 10 μmol reactions with 1 μmol catalyst, 3 equiv. base, 0.1 M concentration
- Customizable Excel Template for quick calculations and easy incorporation into electronic laboratory notebooks
Legal Information
Kit Components Only
- SnapIT Ampule Opener, Regular, for 1-2ml, 5-10ml, 10-15ml ampoules 1 EA
Kit Components Also Available Separately
signalword
Danger
Hazard Classifications
Acute Tox. 4 Dermal - Acute Tox. 4 Inhalation - Aquatic Acute 1 - Aquatic Chronic 1 - Carc. 1B - Eye Dam. 1 - Repr. 1B - Self-heat. 1 - Skin Corr. 1B - STOT RE 2 Oral - STOT SE 3
target_organs
Central nervous system, Kidney,Adrenal gland,Testes, Respiratory system
Storage Class
4.2 - Pyrophoric and self-heating hazardous materials
flash_point_f
-4.0 °F - closed cup
flash_point_c
-20 °C - closed cup
wgk
WGK 3
supp_hazards
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Protocols
Solutions & slurries to make: Go to the online user set-up page to enter molecular weights into the downloadable excel file.
Catalyst screening kits, KitAlysis™, and TLC-MS analysis enable high-throughput synthesis and analysis for efficient reactions.
Protocol for the KitAlysis™ Buchwald-Hartwig Amination Reaction Screening Kit
Articles
All contents in the foil bag are weighed, plated, packed, and sealed in a glove box under nitrogen.
KitAlysis High-Throughput Screening Kits provide solution to efficiently identify or optimize suitable catalytic reaction conditions. Chemist can rapidly run 24 unique micro scale reactions in parallel with tailored conditions.
All of the preformed catalysts used in the kit are air and moisture stable complexes in their commercially available form. Once activated by base under the reaction conditions they become sensitive to air. To best enable scale-up success, the use of standard Schlenk technique is recommended.
Related Content
有机合成中的化学反应设计和优化旨在精确改变反应参数，以达到最佳效果，找到通向目标分子的途径。
Global Trade Item Number
| SKU | GTIN |
|---|---|
| KITALYSIS-CN-1KT | 04061833945223 |