GC Analysis of Pesticides in Wine on SLB®-5ms after SPME using 85 μm Polyacrylate Fiber
Materials
used together
Product No.
Description
Pricing
SPME fiber assembly polyacrylate (PA)
df 85 μm(PA, for use with manual holder, needle size 24 gaCONDITIONS
sample/matrix
white wine spiked with 50 ppb pesticides
SPME fiber
85 μm polyacrylate (57304)
extraction
immersion, room temp (30 min)
desorption process
250 °C for 5 min
column
SLB-5ms, 30 m x 0.25 mm I.D., 0.25 μm (28471-U)
oven
60 °C (1 min), 15 °C/min to 100 °C, 7 °C/min to 300 °C (1 min)
MSD interface
325 °C
scan range
SIM
carrier gas
helium, 0.7 mL/min, constant
liner
0.75 mm I.D. SPME liner
Description
Legal Information
SLB is a registered trademark of Merck KGaA, Darmstadt, Germany