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Merck

28471-U

SLB®-5ms Capillary GC Column

L × I.D. 30 m × 0.25 mm, df 0.25 μm

Synonym(s):

GC column, SPB-5, 5% diphenyl, mass spec

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About This Item

UNSPSC Code:
41115710
NACRES:
SB.54
eCl@ss:
32119290
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material

fused silica

agency

Standard Method 6040D, EN 2005/108/EC, EPA 610,625,8015,8082,8100,8141,8270,OLM04.2 SVOA, EPA TO-13,IP-8,8270,525.2,608.1/608.2,608/8081/OLM04.2 PEST, JMHLW, NIOSH 2530,5503, OSHA 62, meets requirements for USP G27 and G36, suitable for EPA 1613

reg. compliance

FDA LIB 4423

specific analyte(s)

3-MCPD

parameter

-60-340 °C temperature (isothermal), -60-360 °C temperature (programmed)

Beta value

250

df

0.25 μm

technique(s)

GC/MS: suitable, gas chromatography (GC): suitable

L × I.D.

30 m × 0.25 mm

matrix active group

Bonded and highly crosslinked; silphenylene polymer virtually equivalent in polarity to poly(5% diphenyl/95% dimethyl siloxane) phase, SLB 5ms

application(s)

agriculture
chemicals and industrial polymers
cleaning products
clinical
cosmetics
environmental
flavors and fragrances
food and beverages
forensics and toxicology
industrial hygiene
life science and biopharma
personal care
petroleum
pharmaceutical (small molecule)

column type

capillary non-polar

General description

Application: The 5% phenyl equivalent phase provides a boiling point elution order with a slight increase in selectivity, especially for aromatic compounds. The low bleed characteristics, inertness, and durable nature make it the column of choice for environmental analytes (such as semivolatiles, pesticides, PCBs, and herbicides) or anywhere a low bleed non-polar column is required.
USP Code: This column meets USP G27 and G36 requirements.
Phase:
  • Bonded and highly crosslinked
  • Silphenylene polymer virtually equivalent in polarity to poly(5% diphenyl/95% dimethyl siloxane)
Temp. Limits:
  • ≤0.32 mm I.D.: -60 °C to 340 °C (isothermal) or 360 °C (programmed)
  • ≥0.53 mm I.D.: -60 °C to 330 °C (isothermal) or 340 °C (programmed)

Application


  • Determination of propargite, tebuconazole and bromopropylate pesticide residues in Taiwan green jujubes by gas chromatography-tandem mass spectrometry.: This study utilized the SLB-5ms Capillary GC Column to analyze pesticide residues in agricultural produce. The method demonstrated high sensitivity and specificity, highlighting the column′s efficacy in complex sample matrices (Zhang et al., 2014).

  • Characterisation of capillary ionic liquid columns for gas chromatography-mass spectrometry analysis of fatty acid methyl esters.: The research explored the performance of SLB-5ms Capillary GC Columns for the analysis of fatty acid methyl esters. The column exhibited superior resolution and stability, making it a valuable tool for lipid analysis in biochemical applications (Zeng et al., 2013).

Other Notes

We offer a variety of chromatography accessories including analytical syringes

Legal Information

SLB is a registered trademark of Merck KGaA, Darmstadt, Germany


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Protocols

There are three types of analyses: GRO, DRO, and TPH. The published methods are simply variations of these to meet the different analytical needs of the individual agencies.

GC Analysis of PBDE Flame-Retardant Compounds

Example displays how MSTFA/MSTFA-d9 derivatization of amphetamine provides valuable information in mass spectra and chromatograms using SLB-5ms GC column.

Articles

Development and validation of a fatty acid methyl esterification method, using methanolic HCl reagent, for FAME analysis by GC of vegetable oils and fats.

Identification and quantification of the most common extractables originating from single-use equipment by GC/MS and an Extractables and Leachables Screening Standard.

GC Analysis of Neroli Essential Oil on SLB®-5ms

View All Articles

Tommy W McGaha et al.
PloS one, 10(3), e0118904-e0118904 (2015-03-19)
The suite of pheromones that promote communal oviposition by Simulium vittatum, a North American black fly species, was identified and characterized using gas chromatography-mass spectrometry, electrophysiological, and behavioral bioassays. Behavioral assays demonstrated that communal oviposition was induced by egg-derived compounds
Sophie Duclos et al.
Proteomics, 11(5), 854-864 (2011-02-01)
The essential roles of the endovacuolar system in health and disease call for the development of new tools allowing a better understanding of the complex molecular machinery involved in endocytic processes. We took advantage of the floating properties of small
Lisa Simonsson et al.
Chemphyschem : a European journal of chemical physics and physical chemistry, 11(5), 1011-1017 (2010-03-20)
We investigate the Ca(2+)-triggered fusion of lipid vesicles site-selectively tethered to a DNA-modified supported lipid bilayer array, with the DNA strands designed such that hybridization occurs in a zipperlike fashion. Prior to the addition of Ca(2+), which is observed to



Global Trade Item Number

SKUGTIN
28471-U04061835551927